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The influence of grinding on the limestone properties
Pavlík, Tomáš ; Bednárek, Jan (referee) ; Šiler, Pavel (advisor)
This bachelor thesis deals with dry limestone grinding in the vibratory mill and ball mill. Three different limestone samples were used for milling. Samples were ground in the mills without the addition of surfactants. Several methods of grinding were performed in the vibratory mill. At first, the same weight of limestone samples was ground for different grinding time without any interruption except for one case of grinding with breaks for cooling off the grinding tablet. Another method was grinding of different weights of the same sample. The last one used the same weight of different samples. In the ball mill, sample of one type of limestone was ground for various milling time. The particle size, shape of particles, phase composition and crystallite size were studied for the ground samples. Sieve analysis, laser diffraction analysis, scanning electron microscopy, powder X-ray diffraction analysis and X-ray fluorescence analysis were used to determine these properties. For each mill, the amount of energy consumed for limestone grinding was calculated.
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Meta-talc Application in Inorganic Materials
Bednárek, Jan ; Rovnaník, Pavel (referee) ; Palou, Martin (referee) ; Havlica, Jaromír (advisor)
This thesis is focused at possibilities of preparation and characterization of XRD-amorphous delaminated and dehydroxylated talc phase – meta-talc, which can have its potential application and a starter material for a preparation of magnesium-silicate analogues of geopolymers. Changes in structure and morphology of talc ore were observed during this work. For the purposes of this research, two various talc ores – chloritic and dolomitic were examined. Whole process of meta-talc preparation was examined with whole scale of instrumental techniques such as X-ray diffraction, simultaneous thermogravimetric a differential thermal analysis, infrared spectroscopy, scanning electron microscopy or laser analysis of particle size. Meta-talc can be obtained via mechanochemical activation of talc ore with subsequent calcination. Mechanochemical treatment lead to destruction of original crystal structure and breaking of original bonds, i.e. the product of this treatment was almost amorphous and delaminated. Most of hydroxyl groups were converted to molecules of water which remained adsorbed or coordinated in ore structure. These molecules were removed during calcination step.
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Meta-talc Application in Inorganic Materials
Bednárek, Jan ; Rovnaník, Pavel (referee) ; Palou, Martin (referee) ; Havlica, Jaromír (advisor)
This thesis is focused at possibilities of preparation and characterization of XRD-amorphous delaminated and dehydroxylated talc phase – meta-talc, which can have its potential application and a starter material for a preparation of magnesium-silicate analogues of geopolymers. Changes in structure and morphology of talc ore were observed during this work. For the purposes of this research, two various talc ores – chloritic and dolomitic were examined. Whole process of meta-talc preparation was examined with whole scale of instrumental techniques such as X-ray diffraction, simultaneous thermogravimetric a differential thermal analysis, infrared spectroscopy, scanning electron microscopy or laser analysis of particle size. Meta-talc can be obtained via mechanochemical activation of talc ore with subsequent calcination. Mechanochemical treatment lead to destruction of original crystal structure and breaking of original bonds, i.e. the product of this treatment was almost amorphous and delaminated. Most of hydroxyl groups were converted to molecules of water which remained adsorbed or coordinated in ore structure. These molecules were removed during calcination step.
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The influence of grinding on the limestone properties
Pavlík, Tomáš ; Bednárek, Jan (referee) ; Šiler, Pavel (advisor)
This bachelor thesis deals with dry limestone grinding in the vibratory mill and ball mill. Three different limestone samples were used for milling. Samples were ground in the mills without the addition of surfactants. Several methods of grinding were performed in the vibratory mill. At first, the same weight of limestone samples was ground for different grinding time without any interruption except for one case of grinding with breaks for cooling off the grinding tablet. Another method was grinding of different weights of the same sample. The last one used the same weight of different samples. In the ball mill, sample of one type of limestone was ground for various milling time. The particle size, shape of particles, phase composition and crystallite size were studied for the ground samples. Sieve analysis, laser diffraction analysis, scanning electron microscopy, powder X-ray diffraction analysis and X-ray fluorescence analysis were used to determine these properties. For each mill, the amount of energy consumed for limestone grinding was calculated.
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